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Characterization of TiO2/TA(2)O(5) films synthesized by ion beam on NiTi alloy for biomedical applications

Jingxiao LIU , Jihua CHEN , Dazhi YANG , Weiqiang WANG , Yinong WANG , Yingji CAI

材料科学技术(英)

The biocompatibility of implants is determined by their corrosion resistance and surface characteristics. In this study, the surface composition, morphology and microstructure of TiO2/Ta2O5 films synthesized by ion beam enhanced deposition on NiTi alloy were studied. The scratch test results indicate that the interface adhesive strength of TiO2/Ta2O5 film increases with the increasing Ta content. The electrochemical corrosion measurement shows that the TiO2-36%Ta2O5 film is optimal for improving corrosion resistance of NiTi alloy.

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Characterization of Sol-gel-derived TiO2 and TiO2-SiO2 Films for Biomedical Applications

Jingxiao LIU , Fei SHI , Dazhi YANG

材料科学技术(英)

In order to improve the corrosion resistance and biocompatibility of NiTi surgical alloy, TiO2 and TiO2-SiO2 thin films were prepared by sol-gel method. The surface characteristics of the film, which include surface composition, microstructure and surface morphology, were studied by X-ray diffraction (XRD), atomic force microscopy (AFM) and X-ray photoelectron spectra (XPS), respectively. A scratching test was used to assess the interface adhesive strength between the film and substrate. The corrosion resistances of NiTi alloy coated with oxide films were studied by anodic polarization curves measurement in biological solution. Additionally, a preliminary study of the in vitro bioactivity of the films was conducted. The results indicated that TiO2 and TiO2-SiO2 (Ti/Si=4:1) films have higher electrochemical corrosion resistance and can be used as protective layers on NiTi alloy. In addition, TiO2-SiO2 composite films have better bioactivity than TiO2 film.

关键词: TiO2 , null , null , null , null

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